| dc.contributor |
EPSRC - Engineering and Physical Sciences Research Council |
|
| dc.contributor |
NERC - Natural Environment Research Council |
|
| dc.contributor |
Bell, Nicholle |
|
| dc.creator |
Bell, Nicholle |
|
| dc.creator |
Smith, Alan |
|
| dc.creator |
York, Richard |
|
| dc.date |
2022-03-28T10:23:11Z |
|
| dc.date |
2022-04-01T04:15:15Z |
|
| dc.date.accessioned |
2022-05-26T09:24:33Z |
|
| dc.date.available |
2022-05-26T09:24:33Z |
|
| dc.identifier |
Bell, Nicholle; Smith, Alan; York, Richard. (2022). 19F-centred NMR analysis of mono-fluorinated compounds. NMR spectra obtained from 3-fluoro-3-deoxy-D-glucose, [dataset]. University of Edinburgh. School of Chemistry. https://doi.org/10.7488/ds/3422. |
|
| dc.identifier |
https://hdl.handle.net/10283/4381 |
|
| dc.identifier |
https://doi.org/10.7488/ds/3422 |
|
| dc.identifier.uri |
http://localhost:8080/xmlui/handle/CUHPOERS/201068 |
|
| dc.description |
The folder contains raw NMR spectra of 3-fluoro-3-deoxy-D-glucose, which were acquired using Bruker NMR spectrometers using a range of NMR experiments. Dataset is the subject of RSC Advances article entitled 19F-centred NMR analysis of mono-fluorinated compounds.
Specific files are as follows (also listed in summary word document):
1. 400 MHz 1H spectrum of 3-fluoro-3-deoxy-D-glucose, 1.
2. 400 MHz 1H coupled 1D 19F spectrum of 1.
3. 19F-detected z-filtered 2D 1H, 19F HETCOR spectrum of 1.
4. 2D 1H, 19F TOCSY-HETCOR spectrum of 1.
5. 2D 19F, 1H CP-DIPSI3-DIPSI2 spectrum of 1 with FH transfer only.
6. 2D 19F, 1H CP-DIPSI3-DIPSI2 spectrum of 1 with additional HH transfer.
7. 2D 19F, 13C HMBC spectrum optimised for nJFC correlations
8. (3,2)D H1CnF correlation spectrum of 1
9. In phase (3,2)D H1CnF correlation spectrum of 1
10. Antiphase (3,2)D H1CnF correlation spectrum of 1 |
|
| dc.description |
1. 400 MHz 1H spectrum of 3-fluoro-3-deoxy-D-glucose, 1.
2. 400 MHz 1H coupled 1D 19F spectrum of 1.
3. 19F-detected z-filtered 2D 1H, 19F HETCOR spectrum of 1.
4. 2D 1H, 19F TOCSY-HETCOR spectrum of 1.
5. 2D 19F, 1H CP-DIPSI3-DIPSI2 spectrum of 1 with FH transfer only.
6. 2D 19F, 1H CP-DIPSI3-DIPSI2 spectrum of 1 with additional HH transfer.
7. 2D 19F, 13C HMBC spectrum optimised for nJFC correlations
8. (3,2)D H1CnF correlation spectrum of 1
9. In phase (3,2)D H1CnF correlation spectrum of 1
10. Antiphase (3,2)D H1CnF correlation spectrum of 1 |
|
| dc.format |
application/zip |
|
| dc.language |
eng |
|
| dc.publisher |
University of Edinburgh. School of Chemistry |
|
| dc.rights |
Creative Commons Attribution 4.0 International Public License |
|
| dc.subject |
NMR |
|
| dc.subject |
19F |
|
| dc.subject |
glucose |
|
| dc.subject |
mixtures |
|
| dc.subject |
Physical Sciences::Analytical Chemistry |
|
| dc.title |
19F-centred NMR analysis of mono-fluorinated compounds. NMR spectra obtained from 3-fluoro-3-deoxy-D-glucose |
|
| dc.type |
dataset |
|